Detail publikace

Biodegradable WE43 Magnesium Alloy Produced by Selective Laser Melting: Mechanical Properties, Corrosion Behavior, and In-Vitro Cytotoxicity

LOVAŠIOVÁ, P. LOVAŠI, T. KUBÁSEK, J. JABLONSKÁ, E. MSALLAMOVÁ, Š. MICHALCOVÁ, A. VOJTĚCH, D. SUCHÝ, J. KOUTNÝ, D. ALZUBI, E.

Anglický název

Biodegradable WE43 Magnesium Alloy Produced by Selective Laser Melting: Mechanical Properties, Corrosion Behavior, and In-Vitro Cytotoxicity

Typ

článek v časopise ve Web of Science, Jimp

Jazyk

en

Originální abstrakt

In this work, selective laser melting (SLM) technology was used to prepare Mg-4Y-3Nd-Zr (WE43) alloy. This alloy and production method are promising for the design of biodegradable implants. The aim of this study was to investigate the chemical composition, microstructure, mechanical properties, corrosion behavior in simulated body fluid (SBF), and cytotoxicity of the alloy produced by SLM method and to compare it with conventionally gravity cast reference alloy. Analysis of the surface of the revealed an oxygen content of 7 wt.%. Undesirable unmelted and only partially adhered spherical particles of the starting powder were also found. The microstructure of the material was very fine and consisted of alpha-Mg dendritic matrix, beta-Mg-41(Nd, Y)(5) intermetallic phase, Y2O3 inclusions, and 0.6 vol.% of residual porosity. The Vickers hardness, compressive yield strength, compressive strength, and maximum compressive strain were 88 HV0.1, 201 MPa, 394 MPa, and 14%, respectively, which are close to the reference values in as-cast. The in vitro corrosion rates determined by immersion and potentiodynamic tests were 2.6 mm/year and 1.3 mm/year, respectively. Cytotoxicity tests indicated good biocompatibility of the 3D-printed alloy.

Anglický abstrakt

In this work, selective laser melting (SLM) technology was used to prepare Mg-4Y-3Nd-Zr (WE43) alloy. This alloy and production method are promising for the design of biodegradable implants. The aim of this study was to investigate the chemical composition, microstructure, mechanical properties, corrosion behavior in simulated body fluid (SBF), and cytotoxicity of the alloy produced by SLM method and to compare it with conventionally gravity cast reference alloy. Analysis of the surface of the revealed an oxygen content of 7 wt.%. Undesirable unmelted and only partially adhered spherical particles of the starting powder were also found. The microstructure of the material was very fine and consisted of alpha-Mg dendritic matrix, beta-Mg-41(Nd, Y)(5) intermetallic phase, Y2O3 inclusions, and 0.6 vol.% of residual porosity. The Vickers hardness, compressive yield strength, compressive strength, and maximum compressive strain were 88 HV0.1, 201 MPa, 394 MPa, and 14%, respectively, which are close to the reference values in as-cast. The in vitro corrosion rates determined by immersion and potentiodynamic tests were 2.6 mm/year and 1.3 mm/year, respectively. Cytotoxicity tests indicated good biocompatibility of the 3D-printed alloy.

Klíčová slova anglicky

3D printing; selective laser melting; WE43; Mg-alloy; mechanical properties

Vydáno

10.03.2022

Nakladatel

MDPI

Místo

BASEL

ISSN

2075-4701

Ročník

12

Číslo

3

Počet stran

16

BIBTEX


@article{BUT182742,
  author="Patrícia {Lovašiová} and Tomáš {Lovaši} and Jiří {Kubásek} and Eva {Jablonská} and Šárka {Msallamová} and Alena {Michalcová} and Dalibor {Vojtěch} and Jan {Suchý} and Daniel {Koutný} and Enas {Alzubi},
  title="Biodegradable WE43 Magnesium Alloy Produced by Selective Laser Melting: Mechanical Properties, Corrosion Behavior, and In-Vitro Cytotoxicity",
  year="2022",
  volume="12",
  number="3",
  month="March",
  publisher="MDPI",
  address="BASEL",
  issn="2075-4701"
}